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99% Purity Commercial production 2-Methyl-3-nitroanisole 4837-88-1 with Cheapest Price
- Molecular Formula: C8H9NO3
- Molecular Weight: 167.164
- Appearance/Colour: YELLOW TO TAN POWDER OR CRYSTALLINE
- Vapor Pressure: 0.0194mmHg at 25°C
- Melting Point: 54-56 °C(lit.)
- Refractive Index: 1.538
- Boiling Point: 260.9 °C at 760 mmHg
- Flash Point: 121.1 °C
- PSA： 55.05000
- Density: 1.18 g/cm3
- LogP: 2.43500
2-Methyl-3-nitroanisole(Cas 4837-88-1) Usage
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Purification Methods |
2-Methyl-5-nitroanisole crystallises from MeOH (yellow needles) and sublimes in vacuo. [Kuffner Monatsh Chem 91 1152 1960, Beilstein 6 I 178.] |
InChI:InChI=1/C8H9NO3/c1-6-7(9(10)11)4-3-5-8(6)12-2/h3-5H,1-2H3
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4837-88-1 Process route
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861609-40-7
2-methoxy-3-methyl-4-nitro-aniline
-
-
5460-31-1
3-nitro-o-cresol
-
-
4837-88-1
6-methoxy-2-nitrotoluene
Conditions
| Conditions | Yield |
|---|---|
|
With
sulfuric acid; sodium nitrite;
Diazotization;
|
|
|
beim Diazotieren und Verkochen der schwefelsauren Diazoniumloesung;
|
-
-
5460-31-1
3-nitro-o-cresol
-
-
74-88-4
methyl iodide
-
-
4837-88-1
6-methoxy-2-nitrotoluene
Conditions
| Conditions | Yield |
|---|---|
|
With
sodium hydride;
In
N,N-dimethyl-formamide;
|
94%
|
|
With
sodium hydride;
In
N,N-dimethyl-formamide;
at 90 ℃;
for 0.333333h;
|
|
|
3-nitro-o-cresol;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 0 - 20 ℃;
methyl iodide;
In
N,N-dimethyl-formamide; mineral oil;
at 80 ℃;
for 5h;
|
|
|
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 14h;
|
|
|
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 20 ℃;
Inert atmosphere;
|
502 mg
|
4837-88-1 Upstream products
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861609-40-7
2-methoxy-3-methyl-4-nitro-aniline
-
5460-31-1
3-nitro-o-cresol
-
77-78-1
dimethyl sulfate
-
603-83-8
3-nitro-o-tolylamine
4837-88-1 Downstream products
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19689-88-4
2-methoxy-6-nitrobenzaldehyde
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53967-73-0
2-nitro-6-methoxybenzoic acid
-
19500-02-8
2-methyl-3-methoxyaniline
-
4837-89-2
pyruvic acid
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